The final reclaim (reclaim 4) sample was very unique. It had been collected from a rig filled with so much reclaim you couldn’t even pull on it. In an attempt to salvage as much of the reclaim as possible while trying to avoid the use of isopropyl alcohol, I flashed the rig with my torch to lower the viscosity of the oil. I was able to get most to drip out the downstem, and collected it into a No-Goo. This sample then sat in the same non-stick container for over six months. When we decided to do this experiment, I thought this sample would be a good candidate. When I opened the container, the consistency was unlike all of the other samples. This sample of reclaim had turned back into a shatter like consistency, breaking and splintering when handled. It was completely black and stable at room temp, with no discernable odor. Max THC for this “shatterclaim” was only 23.3%, with the Max CBD at 1.7%, both on the low end across all tested samples. What was interesting was the extremely high amount of CBN, which was 8.6%. Out of the four samples, this one had the least amount of total measured cannabinoids, at 33.7% total. 97% of those cannabinoids were decarbed.