Argonne's Advanced Photon Source.

The first analysis of space dust collected by a special collector onboard NASA's Stardust mission and sent back to Earth for study in 2006 suggests the tiny specks open a door to studying the origins of the solar system and possibly the origin of life itself.

This is the first time synchrotron light sources have been used to look at microscopic particles caught in the path of a comet. The Advanced Photon Source, the Advanced Light Source, and the National Synchrotron Light Source at the U.S. Department of Energy's Argonne, Lawrence Berkeley and Brookhaven National Laboratories, respectively, enabled analysis that showed that the dust, which likely originated from beyond our solar system, is more complex in composition and structure than previously imagined.

"Fundamentally, the solar system and everything in it was ultimately derived from a cloud of interstellar gas and dust," says Andrew Westphal, physicist at the University of California, Berkeley's Space Sciences Laboratory and lead author on the paper published this week in Science titled "Evidence for interstellar origin of seven dust particles collected by the Stardust spacecraft". "We're looking at material that's very similar to what made our solar system."

The analysis tapped a variety of microscopy techniques including those that rely on synchrotron radiation. "Synchrotrons are extremely bright light sources that enable light to be focused down to the small size of these particles while providing unprecedented chemical identification," said Hans Bechtel, principal scientific engineering associate at Berkeley Lab.

The APS helped the researchers create a map of the locations and abundances of the different elements in each tiny particle, said Argonne physicist Barry Lai, who was involved with the analysis at the APS.

"The Advanced Photon Source was unique in the capability to perform elemental imaging and analysis on such small particles—just 500 nanometers or less across," Lai said. (That is so small that about 1,000 of them could fit in the period at the end of a sentence.) "This provided an important screening tool for differentiating the origin of each particle."

Researchers used the scanning transmission x-ray and Fourier transform infrared microscopes at the ALS. The X-ray microscope ruled out tens of interstellar dust candidates because they contained aluminum, not found in space or other substances and possibly knocked off the spacecraft and embedded in the aerogel. The infrared spectroscopy helped to identify sample contamination that could ultimately be subtracted later.

"Almost everything we've known about interstellar dust has previously come from astronomical observations—either ground-based or space-based telescopes," says Westphal. But telescopes don't tell you about the diversity or complexity of interstellar dust, he says. "The analysis of these particles captured by Stardust is our first glimpse into the complexity of interstellar dust, and the surprise is that each of the particles are quite different from each other."

Westphal, who is also affiliated with Berkeley Lab's Advanced Light Source, and his 61 co-authors, including researchers from the University of Chicago and the Chicago Field Museum of Natural History, found and analyzed a total of seven grains of possible interstellar dust and presented preliminary findings. All analysis was non-destructive, meaning that it preserved the structural and chemical properties of the particles. While the samples are suspected to be from beyond the solar system, he says, potential confirmation of their origin must come from subsequent tests that will ultimately destroy some of the particles.

"Despite all the work we've done, we have limited the analyses on purpose," Westphal explains. "These particles are so precious. We have to think very carefully about what we do with each particle."

Between 2000 and 2002, the Stardust spacecraft, on its way to meet a comet named Wild 2, exposed the special collector to the stream of dust coming from outside our solar system. The mission objectives were to catch particles from both the comet coma as well as from the interstellar dust stream. When both collections were complete, Stardust launched its sample capsule back to earth where it landed in northwestern Utah. The analyses of Stardust's cometary sample have been widely published in recent years, and the comet portion of the mission has been considered a success.

This new analysis is the first time researchers have looked at the microscopic particles collected en route to the comet. Both types of dust were captured by the spacecraft's sample-collection trays, made of an airy material called aerogel separated by aluminum foil. Three of the space-dust particles (a tenth the size of comet dust) either lodged or vaporized within the aerogel while four others produced pits in the aluminum foil leaving a rim residue that fit the profile of interstellar dust.

Much of the new study relied on novel methods and techniques developed specifically for handling and analyzing the fine grains of dust, which are more than a thousand times smaller than a grain of sand. These methods are described in twelve other papers available now and next week in the journal of Meteoritics & Planetary Science.

One of the first research objectives was to simply find the particles within the aerogel. The aerogel panels were essentially photographed in tiny slices by changing the focus of the camera to different depths, which resulted in millions of images eventually stitched together into video. With the help of a distributed science project called Stardust@home, volunteer space enthusiasts from around the world combed through video, flagging tracks they believed were created by interstellar dust. More than 100 tracks have been found so far, but not all of these have been analyzed. Additionally, only 77 of the 132 aerogel panels have been scanned. Still, Westphal doesn't expect more than a dozen particles of interstellar dust will be seen.

The researchers found that the two larger dust particles from the aerogel have a fluffy composition, similar to that of a snowflake, says Westphal. Models of interstellar dust particles had suggested a single, dense particle, so the lighter structure was unexpected. They also contain crystalline material called olivine, a mineral made of magnesium, iron, and silicon, which suggest the particles came from disks or outflows from other stars and were modified in the interstellar medium.

Three of the particles found in the aluminum foil were also complex, and contain sulfur compounds, which some astronomers believe should not occur in interstellar dust particles. Study of further foil-embedded particles could help explain the discrepancy.

Westphal says that team will continue to look for more tracks as well as take the next steps in dust analysis. "The highest priority is to measure relative abundance of three stable isotopes of oxygen," he says. The isotope analysis could help confirm that the dust originated outside the solar system, but it's a process that would destroy the precious samples. In the meantime, Westphal says, the team is honing their isotope analysis technique on artificial dust particles called analogs. "We have to be super careful," he says. "We're doing a lot of work on analogs to practice, practice, practice."

The Advanced Photon Source is currently in the process of designing a proposed upgrade that would increase its ability to do such analyses, Lai said.

"With the APS upgrade, we would be able to increase the spatial resolution and to image faster—effectively scanning a larger area of the aerogel in a shorter time," he said.

Since just over half of the aerogels have been checked for particles, there are plenty more waiting to be analyzed.

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